L-(-)-二苯甲酰酒石酸合成路线 （共 16 条）
反应条件
in ethanol T=5 - 20°C; 16 h; Resolution of racemate; Purification / work up;
参考文献
WO2008/12046 A1, ;
Page/Page column 10 ;
反应条件
chiral stationary phase including (R)-naphthylethyl-carbamate-functionalized CF6 in methanol; acetic acid; triethylamine; acetonitrile T=20°C; Resolution of racemate; Purification / work up;
参考文献
Sun, Ping; Wang, Chunlei; Breitbach, Zachary S.; Zhang, Ying; Armstrong, Daniel W.
Analytical Chemistry, 2009 , vol. 81, # 24 p. 10215 - 10226
参考文献
Mravik, Andras; Lepp, Zsolt; Fogassy, Elemer
Tetrahedron Asymmetry, 1996 , vol. 7, # 8 p. 2387 - 2390
Title/Abstract Full Text View citing articles Show Details
Elekes, Ferenc; Kovari, Zoltan; Mravik, Andras; Boecskei, Zsolt; Fogassy, Elemer
Tetrahedron Asymmetry, 1998 , vol. 9, # 16 p. 2895 - 2900
反应条件
in methanol; isopropyl alcohol 1 h; RefluxResolution of racemate;
参考文献
Divi's Laboratories Limited
Patent: US2012/197022 A1, 2012 ;
Location in patent: Page/Page column 4 ;
反应条件
in acetone T=35 - 40°C; 27 h; Resolution of racemate; Purification / work up;
参考文献
GRUeNENTHAL GMBH
Patent: WO2008/12047 A1, 2008 ;
Location in patent: Page/Page column 19 ;
反应条件
in anhydrous xylene
T=140°C; 3 h; Dean-Stark trap;
参考文献
Ruskowski, Pawel; Synoradzki, Ludwik; Wlostowski, Marek
Arkivoc, 2011 , vol. 2011, # 9 p. 142 - 154
