2-氨基-1-呋喃-2-基-乙醇合成路线 （共 8 条）
反应条件
hydrogen; palladium on activated charcoal in methanol 24 h;
参考文献
Haukaas, Michael H.; Li, Miaosheng; Starosotnikov, Alexey M.; O'Doherty, George A.
Heterocycles, 2008 , vol. 76, # 2 p. 1549 - 1559
反应条件
1.1: LiAlH4 / tetrahydrofuran / 0.5 h / 0 °C 1.2: 85 percent / tetrahydrofuran / 30 h 2.1: hydrogen / Pd/C / methanol / 24 h View Scheme
参考文献
Haukaas, Michael H.; O'Doherty, George A.
Organic Letters, 2001 , vol. 3, # 24 p. 3899 - 3902
反应条件
lithium aluminium tetrahydride in diethyl ether 8 h; Heating;
参考文献
Demir; Tanyeli; Aksoy; Gulbeyaz; Mahasneh
Synthesis, 1995 , # 9 p. 1071 - 1073
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; N,N-dimethyl-formamide 48 h; Ambient temperature;
参考文献
Tsuge, Otohiko; Kanemasa, Shuji; Hatada, Akira; Matsuda, Koyo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 2537 - 2546
反应条件
1: sodium tetrahydroborate / methanol / 1.25 h / 5 - 20 °C / |Green chemistry 2: hydrogen; palladium 10 on activated carbon / methanol / 2 h / 30 °C / 7500.75 Torr / |Green chemistry View Scheme
参考文献
Schrittwieser, Joerg H.; Coccia, Francesca; Kara, Selin; Grischek, Barbara; Kroutil, Wolfgang; D'Alessandro, Nicola; Hollmann, Frank
Green Chemistry, 2013 , vol. 15, # 12 p. 3318 - 3331
反应条件
1: sodium azide; potassium iodide / water; acetonitrile / 1 h / 60 °C / |Green chemistry 2: sodium tetrahydroborate / methanol / 1.25 h / 5 - 20 °C / |Green chemistry 3: hydrogen; palladium 10 on activated carbon / methanol / 2 h / 30 °C / 7500.75 Torr / |Green chemistry View Scheme
参考文献
Schrittwieser, Joerg H.; Coccia, Francesca; Kara, Selin; Grischek, Barbara; Kroutil, Wolfgang; D'Alessandro, Nicola; Hollmann, Frank
Green Chemistry, 2013 , vol. 15, # 12 p. 3318 - 3331
反应条件
1: bromine / diethyl ether; 1,4-dioxane / 16 h / 5 - 20 °C / |Inert atmosphere; |Green chemistry 2: sodium azide; potassium iodide / water; acetonitrile / 1 h / 60 °C / |Green chemistry 3: sodium tetrahydroborate / methanol / 1.25 h / 5 - 20 °C / |Green chemistry 4: hydrogen; palladium 10 on activated carbon / methanol / 2 h / 30 °C / 7500.75 Torr / |Green chemistry View Scheme
参考文献
Schrittwieser, Joerg H.; Coccia, Francesca; Kara, Selin; Grischek, Barbara; Kroutil, Wolfgang; D'Alessandro, Nicola; Hollmann, Frank
Green Chemistry, 2013 , vol. 15, # 12 p. 3318 - 3331
反应条件
1.1: benzene / 33 - 35 °C 1.2: |Reflux 2.1: sodium hydroxide / 0 - 5 °C View Scheme
参考文献
Ye, Fei; Liu, Cheng-Guo; Wang, Xin-Ming; Fu, Ying; Gao, Shuang
Heterocyclic Communications, 2013 , vol. 19, # 3 p. 201 - 205
