反应条件
1: pyridine / CH2Cl2 / 0.5 h / 0 °C 2: n-BuLi / hexane; tetrahydrofuran / 18 h / Ambient temperature 3: 92 percent / K2Os2(OH)4, (DHQD)2PHAL, K2CO3, potassium ferricyanate, CH3SO2NH2 / H2O; 2-methyl-propan-2-ol / 96 h / Ambient temperature 4: 1) CH3SO2Cl, pyridine, 2) K2CO3 / 1) CH2Cl2, RT, 2) aq. CH3OH, RT, 18 h View Scheme
参考文献
Tomkinson, Nicholas C. O.; Willson, Timothy M.; Russel, Jonathon S.; Spencer, Thomas A.
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9919 - 9923
