2-溴-5,6-二甲氧基-1-茚酮合成路线 (共 4 条)
反应条件
copper(I) bromide; copper(ll) bromide in chloroform; ethyl acetate Reflux;
参考文献
O'Brien, Christopher J.; Nixon, Zachary S.; Holohan, Andrew J.; Kunkel, Stephen R.; Tellez, Jennifer L.; Doonan, Bryan J.; Coyle, Emma E.; Lavigne, Florie; Kang, Lauren J.; Przeworski, Katherine C.
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15281 - 15289
反应条件
in ethanol; chloroform
参考文献
Akzo N.V.
Patent: US4705782 A1, 1987 ;
反应条件
potassium tert-butylate in dimethyl sulfoxide T=15 - 20°C; Darzens condensation; Inert atmosphere;
参考文献
Dubey, Shailendra Kumar; Kharbanda, Manita; Dubey, Sushil Kumar; Mathela, Chandra Shekhar
Chemical and Pharmaceutical Bulletin, 2010 , vol. 58, # 9 p. 1157 - 1160
反应条件
n-butyllithium in tetrahydrofuran T=-78°C; Darzens condensation; Inert atmosphere;
参考文献
Dubey, Shailendra Kumar; Kharbanda, Manita; Dubey, Sushil Kumar; Mathela, Chandra Shekhar
Chemical and Pharmaceutical Bulletin, 2010 , vol. 58, # 9 p. 1157 - 1160