反应条件
in pentane
N2 atmosphere; addn. of soln. of (Me2BS)2 to soln. of N(BCl2)3 (molar ratio 1:1., dropwise, -78°C, stirring), warming to room temp. (12 h); removal of solvent (vac.), distn. (10.8 Pa, 33°C); solid residue sublimed (80°C, 1.3 Pa) yield (ClBS2)2BN; elem. anal.;
参考文献
Kendrick, Aidan; Noeth, Heinrich; Stalla, Beate; Storch, Wolfgang
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 1311 - 1320
