2-甲氧基-4-氨基苯甲酸甲酯合成路线 （共 39 条）
反应条件
nickel Hydrogenation;
参考文献
Clinton et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 592,595
反应条件
potassium hydroxide in acetone T=25°C; 4 h;
参考文献
Chiron, Julien; Galy, Jean-Pierre
Heterocycles, 2003 , vol. 60, # 7 p. 1653 - 1672
参考文献
American Cyanamid Company
Patent: US5753648 A1, 1998 ;
US 5753648 A
反应条件
thionyl chloride T=0°C; Heating / reflux;
参考文献
Chakravarty, Sarvajit; Dugar, Sundeep; Lu, Qing; Luedtke, Gregory R.; Mavunkel, Babu J.; Perumattam, John J.; Tester, Richland W.
Patent: US2004/142940 A1, 2004 ;
Location in patent: Page/Page column 70 ;
US 20040142940 A1
反应条件
potassium acetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl acetamide T=120°C;
参考文献
Jia, Yanxing; Zhu, Jieping
Journal of Organic Chemistry, 2006 , vol. 71, # 20 p. 7826 - 7834
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; 3 h; Inert atmosphere;
参考文献
Terai, Takuya; Ito, Hiroki; Kikuchi, Kazuya; Nagano, Tetsuo
Chemistry - A European Journal, 2012 , vol. 18, # 24 p. 7377 - 7381
反应条件
1: 100 percent / diethyl ether / 0.33 h / 25 °C 2: 1.) LiH / 1.) THF, RT, 15 min, 2.) THF, 65 deg C, 1 h View Scheme
参考文献
Terai, Takuya; Ito, Hiroki; Kikuchi, Kazuya; Nagano, Tetsuo
Chemistry - A European Journal, 2012 , vol. 18, # 24 p. 7377 - 7381
反应条件
1: potassium carbonate / acetone / 5 h / Reflux 2: palladium 10 on activated carbon; hydrogen / methanol / 3 h / 20 °C / Inert atmosphere View Scheme
参考文献
Terai, Takuya; Ito, Hiroki; Kikuchi, Kazuya; Nagano, Tetsuo
Chemistry - A European Journal, 2012 , vol. 18, # 24 p. 7377 - 7381
反应条件
1: dioxane; diethyl ether 2: diethyl ether; methanol 3: SnCl2; concentrated aqueous HCl View Scheme
参考文献
Hueckel; Janecka
Archiv der Pharmazie (Weinheim, Germany), 1951 , vol. 284, p. 341,346
反应条件
1: diethyl ether; methanol 2: SnCl2; concentrated aqueous HCl View Scheme
参考文献
Hueckel; Janecka
Archiv der Pharmazie (Weinheim, Germany), 1951 , vol. 284, p. 341,346
