反应条件
in acetonitrile the soln. in CH3CN was stirred for 2 h at room temp. (Ar); the solvent was removed in vac., the residue was treated with THF, filtered, concd., diethyl ether layered for 4 days, crystals were filtered, washed with THF-diethyl ether, dried in vac.; elem. anal.;
参考文献
Lang, Jian-Ping; Kawaguchi, Hiroyuki; Tatsumi, Kazuyuki
Journal of the Chemical Society, Dalton Transactions, 2002 , # 12 p. 2573 - 2580
