三(2-苯基苯基)亚磷酸酯合成路线 (共 4 条)
反应条件
triethylamine; phosphorus trichoride in toluene 18 h; Heating;
参考文献
Bedford, Robin B.; Hazelwood, Samantha L. Welch; Horton, Peter N.; Hursthouse, Michael B.
Journal of the Chemical Society. Dalton Transactions, 2003 , # 21 p. 4164 - 4174
反应条件
N-ethyl-N,N-diisopropylamine; phosphorus trichoride in toluene T=-20 - 20°C; 14 h;
参考文献
Swennenhuis, Bert H. G.; Chen, Ruifang; Van Leeuwen, Piet W. N. M.; De Vries, Johannes G.; Kamer, Paul C. J.
Organic Letters, 2008 , vol. 10, # 5 p. 989 - 992
反应条件
phosphorus trichoride T=120°C; 6 h;
参考文献
Bergbreiter, David E.; Chandran, Rama
Journal of Organic Chemistry, 1986 , vol. 51, # 25 p. 4754 - 4760
反应条件
in diethyl ether under Ar; reaction with 1 equiv of P(OC6H4-o-Ph)3 at -30°C to room temp.;
参考文献
Benn, R.; Buessemeier, B.; Holle, S.; Jolly, P. W.; Mynott, R.; et all.
Journal of Organometallic Chemistry, 1985 , vol. 279, p. 63 - 86