反应条件
1.1: sodium tetrahydroborate / isopropyl alcohol / 2 h / 3 - 20 °C 2.1: acetonitrile / |Reflux 3.1: sodium hydride / 1,4-dioxane; mineral oil / 1 h / 20 °C / |Inert atmosphere; |Reflux 3.2: |Inert atmosphere; |Reflux 4.1: nitric acid / acetone / 12 h View Scheme
参考文献
Dulcevscaia, Galina M.; Kravtsov, Victor Ch.; Macaev, Fliur Z.; Duca, Gheorghe G.; Stingachi, Eugenia P.; Pogrebnoi, Serghei I.; Boldescu, Veaceslav V.; Clapco, Steliana F.; Tiurina, Janeta P.; Deseatnic-Ciloci, Alexandra A.; Lipkowski, Janusz; Liu, Shi-Xia; Decurtins, Silvio; Baca, Svetlana G.
Polyhedron, 2013 , vol. 52, p. 106 - 114