2,6-二甲基吡啶-3,5-二羧酸二甲酯合成路线 （共 18 条）
反应条件
urea-hydrogen peroxide; iodine in ethyl acetate
T=20°C; 5 h;
参考文献
Filipan-Litvic, Mirela; Litvic, Mladen; Vinkovic, Vladimir
Tetrahedron, 2008 , vol. 64, # 24 p. 5649 - 5656
反应条件
oxygen; isobutyraldehyde; C39H45N12O3Fe in 1,2-dichloro-ethane
T=20°C; P=760 Torr; 72 h;
参考文献
Saalfrank; Reihs; Hug
Tetrahedron Letters, 1993 , vol. 34, # 38 p. 6033 - 6036
反应条件
tert.-butylhydroperoxide; chlorophthalocyaninato(2-)ferrate(III); acetic acid
T=20°C; 0.05 h;
参考文献
Filipan-Litvic, Mirela; Litvic, Mladen; Vinkovic, Vladimir
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 20 p. 9276 - 9282
反应条件
molybdenium(VI) oxotetrachloride in acetonitrile
0.25 h; Reflux;
参考文献
Litvic, Mladen; Regovic, Maja; Smic, Karolina; Lovric, Marija; Filipan-Litvic, Mirela
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 11 p. 3676 - 3681
反应条件
cobalt naphthenate; oxygen in chloroform
2.5 h; Heating;
参考文献
Chavan, Subhash P.; Kharul, Rajendra K.; Kalkote, Uttam R.; Shivakumar
Synthetic Communications, 2003 , vol. 33, # 8 p. 1333 - 1340
反应条件
sodium cyanide in N,N-dimethyl-formamide
T=60°C; 0.333333 h;
参考文献
McInally, Thomas; Tinker, Alan C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1837 - 1844
反应条件
tert.-butylhydroperoxide; chlorophthalocyaninato(2-)ferrate(III); acetic acid
T=20°C; 0.05 h;
参考文献
Filipan-Litvic, Mirela; Litvic, Mladen; Vinkovic, Vladimir
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 20 p. 9276 - 9282
反应条件
KBrO3; iron(III) chloride in water; acetonitrile
0.166667 h; Heating;
参考文献
Zeynizadeh, Behzad; Dilmaghani, Karim Akbari; Roozijoy, Asli
Journal of Chemical Research, 2005 , # 10 p. 657 - 658
反应条件
1: 13.7 percent / ammonium acetate / aq. ethanol; various solvent(s) / 140 h / 20 °C / n
2: 71 percent / Pb(OAc)4 / CH2Cl2; acetic acid / 0.5 h / 20 °C
View Scheme
参考文献
Litvic, Mladen; Cepanec, Ivica; Filipan, Mirela; Kos, Karmen; Bartolincic, Anamarija; Druskovic, Vinka; Tibi, Mohamed Majed; Vinkovic, Vladimir
Heterocycles, 2005 , vol. 65, # 1 p. 23 - 35
反应条件
ammonium chlorate
T=80°C; Hantzsch pyridine synthesis; 3.33333 h; Neat (no solvent);
参考文献
Nasr-Esfahani, Masoud; Karami, Bahador; Behzadi, Masoume
Journal of Heterocyclic Chemistry, 2009 , vol. 46, # 5 p. 931 - 935
