2,6-二甲基吡啶-3,5-二羧酸二甲酯合成路线 （共 18 条）
反应条件
sodium perchlorate in acetonitrile
Electrochemical reaction;
参考文献
Turovska; Goba; Turovskis; Grinberga; Belyakov; Stupnikova; Liepinsh; Stradins
Chemistry of Heterocyclic Compounds, 2008 , vol. 44, # 12 p. 1483 - 1490
反应条件
sodium perchlorate in acetonitrile
Electrochemical reaction;
参考文献
Turovska; Goba; Turovskis; Grinberga; Belyakov; Stupnikova; Liepinsh; Stradins
Chemistry of Heterocyclic Compounds, 2008 , vol. 44, # 12 p. 1483 - 1490
参考文献
Pendleton, Max D.; Beddoes, Roy L.; Andrew, Nell J.; Butters, Michael; Joule, John A.
Journal of Chemical Research, Miniprint, 1997 , # 3 p. 616 - 642
反应条件
Electrochemical reaction;
参考文献
Turovska; Goba; Turovskis; Grinberga; Belyakov; Stupnikova; Liepinsh; Stradins
Chemistry of Heterocyclic Compounds, 2008 , vol. 44, # 12 p. 1483 - 1490
反应条件
potassium phosphate; ethylenediaminetetraacetic acid; Emulgen 911; human liver cytochrome b5; human liver HL 39 lipid extract; rabbit liver NADPH-P-450 reductase; yeast P-450 IIIA4; magnesium chloride in water
other human liver enzymes; Rate constant;
参考文献
Guengerich; Brian; Iwasaki; Sari; Baarnhielm; Berntsson
Journal of Medicinal Chemistry, 1991 , vol. 34, # 6 p. 1838 - 1844
反应条件
pyridine; thionyl chloride
1.) CH2Cl2, from 0 deg C to 20 deg C, 1 h, 2.) CH2Cl2, 20 deg C, 18 h; Multistep reaction;
参考文献
Eynde, Jean-Jacques Vanden; Mayence, Annie; Maquestiau, Andre; Anders, Ernst
Heterocycles, 1994 , vol. 37, # 2 p. 815 - 822
反应条件
formaldehyd
Product distribution;
参考文献
Chupp, John P.; Smith, Lowell R.
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 1785 - 1792
反应条件
1: LiAlH4, sodium sulfate / tetrahydrofuran
2: 95 percent / thionyl chloride / 2 h / Ambient temperature
View Scheme
参考文献
Kang,H.C.; Boekelheide,V.
Journal of the American Chemical Society, 1984 , vol. 106, p. 2672
