3,3-氧杂环丁烷二甲醇合成路线 （共 15 条）
反应条件
1: With potassium hydroxide; carbonic acid diethyl ester in ethanol T=135°C; 4 h; 2: T=170 - 190°C; 2 h;
参考文献
Shanghai Yingli Science And Technology Co., Ltd; Shanghai Pharmvally Innovation Institution Of Biomedicine; Shanghai Chempartner Co., Ltd; XU, Zusheng; QIAN, Su
Patent: EP2676965 A1, 2013 ;
Location in patent: Paragraph 0175; 0176 ;
反应条件
potassium hydroxide T=180°C; Erhitzen des Reaktionsgemisches unter vermindertem Druck;
参考文献
The Regents of the University of California
Patent: US6200599 B1, 2001 ;
反应条件
potassium hydroxide in ethanol
参考文献
Korolev; Eremenko; Meshikhina; Aleksandrov; Konovalova; Lodygina
Russian Chemical Bulletin, 2003 , vol. 52, # 8 p. 1859 - 1863
参考文献
Issidorides; Matar
Journal of the American Chemical Society, 1955 , vol. 77, p. 6382
反应条件
potassium hydroxide in ethanol 2 h; Heating;
参考文献
Korolev; Eremenko; Meshikhina
Russian Chemical Bulletin, 2002 , vol. 51, # 12 p. 2306 - 2307
反应条件
potassium hydroxide in ethanol 5 h; Heating; Yield given;
参考文献
Ameduri, Bruno; Boutevin, Bernard; Karam, Lina
Journal of Fluorine Chemistry, 1993 , vol. 65, # 1-2 p. 43 - 48
反应条件
zuletzt unter vermindertem Druck bis auf 200grad;
参考文献
Cheymol et al.
Bulletin de la Societe Chimique de France, 1959 , p. 1184
Full Text Show Details
Pattison
Journal of the American Chemical Society, 1957 , vol. 79, p. 3455
反应条件
zuletzt bei Siedetemperatur;
参考文献
Govaert; Beyaert
Proceedings of the Koninklijke Nederlandse Akademie van Wetenschappen, Series B: Physical Sciences, 1939 , vol. 42, p. 790,792
反应条件
potassium hydroxide
T=190°C;
参考文献
Cheymol et al.
Bulletin de la Societe Chimique de France, 1959 , p. 1184
反应条件
nitric acid; acetic anhydride; acetic acid in chloroform; water
T=-5 - 20°C;
参考文献
Korolev; Eremenko; Meshikhina; Aleksandrov; Konovalova; Lodygina
Russian Chemical Bulletin, 2003 , vol. 52, # 8 p. 1859 - 1863
