(S)-(-)-1-(2-萘基)乙醇合成路线 (共 74 条)
反应条件
(5aS,10bR)-5a,10b-dihydro-2-(pentafluorophenyl)-4H,6H-indeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazinium tetrafluoroborate; 3-benzylriboflavin tetraacetate; triethylamine in toluene T=20°C; 4 h; Resolution of racemateAirMolecular sieve; optical yield given as percent eeenantioselective reaction;
参考文献
Iwahana, Soichiro; Iida, Hiroki; Yashima, Eiji
Chemistry - A European Journal, 2011 , vol. 17, # 29 p. 8009 - 8013
反应条件
C32H31Cl2N4OPRu; potassium isopropoxide T=30°C; P=750.075 Torr; 0.333333 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Ye, Wenjing; Zhao, Miao; Yu, Zhengkun
Chemistry - A European Journal, 2012 , vol. 18, # 35 p. 10843 - 10846
反应条件
(S)-N-(1-(tert-butylcarbamoyl)-1-(4-(dimethylamino)pyridin-3-yl)methyl)-L-valinemethyl ester; triethylamine in toluene T=-78°C; 15 h; enantioselective reaction;
参考文献
Mandai, Hiroki; Irie, Shunsuke; Akehi, Masaru; Yuri, Kazunobu; Yoden, Masaaki; Mitsudo, Koichi; Suga, Seiji
Heterocycles, 2013 , vol. 87, # 2 p. 329 - 340
反应条件
Na-Pi buffer in acetone 48 h; tubers of Helianthus tuberosus presence, pH 5.9; other biologically active material: tubers of Solanum tuberosum cv. Saturna; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mironowicz, Agnieszka
Phytochemistry, 1998 , vol. 47, # 8 p. 1531 - 1534
反应条件
potassium carbonate in methanol Ambient temperature;
参考文献
Laumen, Kurt; Schneider, Manfred P.
Journal of the Chemical Society, Chemical Communications, 1988 , p. 598 - 600
反应条件
1: lipase from candida antartica / aq. phosphate buffer / 48 h / 30 °C 2: sodium hydroxide; water / 2 h / 20 °C View Scheme
参考文献
Kataoka, Noriyuki; Okudomi, Masayuki; Chihara, Naoka; Matsumoto, Kazutsugu
Letters in Organic Chemistry, 2012 , vol. 9, # 9 p. 615 - 621
反应条件
1: lipase from candida antartica / aq. phosphate buffer / 48 h / 30 °C 2: sodium hydroxide; water / 2 h / 20 °C View Scheme
参考文献
Kataoka, Noriyuki; Okudomi, Masayuki; Chihara, Naoka; Matsumoto, Kazutsugu
Letters in Organic Chemistry, 2012 , vol. 9, # 9 p. 615 - 621
反应条件
water; sodium hydroxide T=20°C; 2 h;
参考文献
Kataoka, Noriyuki; Okudomi, Masayuki; Chihara, Naoka; Matsumoto, Kazutsugu
Letters in Organic Chemistry, 2012 , vol. 9, # 9 p. 615 - 621
反应条件
water; sodium hydroxide T=20°C; 2 h;
参考文献
Kataoka, Noriyuki; Okudomi, Masayuki; Chihara, Naoka; Matsumoto, Kazutsugu
Letters in Organic Chemistry, 2012 , vol. 9, # 9 p. 615 - 621
反应条件
phosphate buffer in diethyl ether 12 h; Ambient temperaturebovine liver acetone powder (BLAP); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Basavaiah, Deevi; Krishna, Peddinti Rama
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 1 p. 131 - 134