(S)-(-)-1-(2-萘基)乙醇合成路线 （共 74 条）
反应条件
roots of Daucus carota L in phosphate buffer; acetone pH=6.5; 48 h; Title compound not separated from byproducts;
参考文献
Mczka, Wanda K; Mironowicz, Agnieszka
Tetrahedron Asymmetry, 2002 , vol. 13, # 21 p. 2299 - 2302
反应条件
Candida antarctica lipase B in tert-butyl methyl ether 16 h; Enzymatic reaction; optical yield given as percent ee;
参考文献
Brossat, Maude; Moody, Thomas S.; Nanteuil, Florian De; Taylor, Stephen J.C.; Vaughan, Fatima
Organic Process Research and Development, 2009 , vol. 13, # 4 p. 706 - 709
反应条件
sodium hydroxide; (S)-1-(2-diphenylphosphino-1-naphthyl)isoquinoline rhodium; dihydrogen peroxide; benzo[1,3,2]dioxaborole 1.) THF, RT, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Valk, Jean Marc; Whitlock, Gavin A.; Layzell, Timothy P.; Brown, John M.
Tetrahedron: Asymmetry, 1995 , vol. 6, # 10 p. 2593 - 2596
反应条件
(S)-(4-tert-butyl-2-thioxothiazolidin-3-yl)[4-(dimethylamino)pyridin-3-yl]methanone; 2,3,5-trimethyl-pyridine in diethyl ether T=0°C; 3 h; Product distribution; Further Variations:CatalystsSolventsTemperatures;
参考文献
Yamada, Shinji; Misono, Tomoko; Iwai, Yuko; Masumizu, Ayako; Akiyama, Yukiko
Journal of Organic Chemistry, 2006 , vol. 71, # 18 p. 6872 - 6880
反应条件
magnesium 1.) ether, reflux, 2.) r.t., overnight; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Janssen; Klunder; Zwanenburg
Tetrahedron, 1991 , vol. 47, # 36 p. 7645 - 7662
反应条件
sodium tetrahydroborate in solid 120 h; Ambient temperature; Product distribution;
参考文献
Toda, Fumio; Shigemasa, Tatsuya
Carbohydrate Research, 1989 , vol. 192, p. 363 - 365
参考文献
Yan, Hailong; Jang, Hyeong Bin; Lee, Ji-Woong; Kim, Hong Ki; Lee, Soon Won; Yang, Jung Woon; Song, Choong Eui
Angewandte Chemie - International Edition, 2010 , vol. 49, # 47 p. 8915 - 8917
反应条件
1: diphenylphosphoryl azide / toluene / 16 h / 20 °C 2: 961 mg / LiAlH4 / diethyl ether / a) reflux, 2 h, b) 20 deg C, 12 h View Scheme
参考文献
Occhiato, Ernesto; Jones, J. Bryan
Tetrahedron, 1996 , vol. 52, # 12 p. 4199 - 4214
反应条件
[Cp*Ru(ICy)Cl]; sodium t-butanolate in toluene T=20°C;
参考文献
Bosson, Johann; Nolan, Steven P.
Journal of Organic Chemistry, 2010 , vol. 75, # 6 p. 2039 - 2043
反应条件
[Ir(η5-C5Me5)(C6H4-2-CH2NHCH3)(NCCH3)](PF6); potassium tert-butylate in toluene T=20°C; 3.33333 h; Inert atmosphere;
参考文献
Jerphagnon, Thomas; Gayet, Arnaud J.A.; Berthiol, Florian; Ritleng, Vincent; Mrsic, Natasa; Meetsma, Auke; Pfeffer, Michel; Minnaard, Adriaan J.; Feringa, Ben L.; De Vries, Johannes G.
Chemistry - A European Journal, 2009 , vol. 15, # 46 p. 12780 - 12790
