(S)-(-)-1-(2-萘基)乙醇合成路线 （共 74 条）
反应条件
1: diphenylphosphoryl azide / toluene / 16 h / 20 °C 2: 961 mg / LiAlH4 / diethyl ether / a) reflux, 2 h, b) 20 deg C, 12 h View Scheme
参考文献
Occhiato, Ernesto; Jones, J. Bryan
Tetrahedron, 1996 , vol. 52, # 12 p. 4199 - 4214
反应条件
1: diphenylphosphoryl azide / toluene / 16 h / 20 °C 2: 961 mg / LiAlH4 / diethyl ether / a) reflux, 2 h, b) 20 deg C, 12 h View Scheme
参考文献
Occhiato, Ernesto; Jones, J. Bryan
Tetrahedron, 1996 , vol. 52, # 12 p. 4199 - 4214
反应条件
[Ir(η5-C5Me5)(C6H4-2-CH2NHCH3)(NCCH3)](PF6); potassium tert-butylate in toluene T=20°C; 3.33333 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 46 p. 12780 - 12790
反应条件
bromine; 1,2-bis-(diphenylphosphino)ethane in dichloromethane
T=0 - 25°C;
参考文献
Richman, Jack E.
Tetrahedron Letters, 2010 , vol. 51, # 21 p. 2793 - 2796
