4-氨基-2-甲基-3-硝基吡啶合成路线 (共 4 条)
参考文献
G. D. Searle and Co.
Patent: US5302601 A1, 1994 ;
US 5302601 A
反应条件
sulfuric acid; nitric acid in water T=65°C; 3 h;
参考文献
Tite, Tony; Lougiakis, Nikolaos; Marakos, Panagiotis; Pouli, Nicole
Synlett, 2009 , # 18 p. 2927 - 2930
反应条件
nickel monoaluminide in methanol
参考文献
G. D. Searle and Co.
Patent: US5302601 A1, 1994 ;
US 5302601 A
反应条件
1: 98 percent / 3 h / Heating 2: 61 percent / 85percent aq. m-chloroperbenzoic acid / CHCl3 / 15 h / Ambient temperature 3: 51 percent / N,N-dimethylformamide / 12 h / 90 °C 4: 49 percent / H2 / Raney nickel / methanol / 2 h / Ambient temperature 5: 25 percent / aq. sodium hydroxide / 3 h / Heating View Scheme
参考文献
Mahadevan,Indumathy; Rasmussen, Malcolm
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 2 p. 359 - 367