1: With sodium hydrogencarbonate in ethanol 6 h; Heating / reflux; 2: With sodium hydroxide in 1,4-dioxane; water T=20°C;
参考文献
CALIFORNIA PACIFIC MEDICAL CENTER; CATHOLIC HEALTHCARE WEST, d.b.a ST. MARY'S MEDICAL CENTER
Patent: WO2003/101998 A1, 2003 ;
Location in patent: Page 40-42 ;
potassium carbonate in dimethyl sulfoxide T=100°C; 63 h;
参考文献
Lauteslager, Xavier Y.; Van Stokkum, Ivo H. M.; Van John Ramesdonk; Bebelaar, Dick; Fraanje, Jan; Goubitz, Kees; Schenk, Henk; Brouwer, Albert M.; Verhoeven, Jan W.
European Journal of Organic Chemistry, 2001 , # 16 p. 3105 - 3118
1: 90 percent / K2CO3 / dimethylsulfoxide / 8 h / 90 °C 2: 82 percent / SnCl2*H2O / ethyl acetate / 2 h / Heating View Scheme
参考文献
Lauteslager, Xavier Y.; Van Stokkum, Ivo H. M.; Van John Ramesdonk; Bebelaar, Dick; Fraanje, Jan; Goubitz, Kees; Schenk, Henk; Brouwer, Albert M.; Verhoeven, Jan W.
European Journal of Organic Chemistry, 2001 , # 16 p. 3105 - 3118
