1: diisopropylamine With n-butyllithium in tetrahydrofuran T=-78 - 20°C; 1 h; 2: 2-chlorophenyl trifluoromethanesulfonate in tetrahydrofuran T=-78 - 20°C; 0.166667 h; Further stages. Title compound not separated from byproducts.;
参考文献
Charmant, Jonathan P. H.; Dyke, Alan M.; Lloyd-Jones, Guy C.
Chemical Communications, 2003 , # 3 p. 380 - 381