6-甲氧基-alpha-甲基-2-萘乙醛合成路线 (共 35 条)
反应条件
potassium permanganate; magnesium sulfate in acetone 2 h;
参考文献
Shishido, Kozo; Yamashita, Akitake; Hiroya, Kou; Fukumoto, Keiichiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 469 - 475
反应条件
ethanol; horse liver alcohol dehydrogenase; NADH dipotassium salt in tetrahydrofuran pH=8; 24 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Galletti, Paola; Emer, Enrico; Gucciardo, Gabriele; Quintavalla, Arianna; Pori, Matteo; Giacomini, Daria
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 18 p. 4117 - 4123
反应条件
ethanol; horse liver alcohol dehydrogenase; NADH dipotassium salt pH=8; 24 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Galletti, Paola; Emer, Enrico; Gucciardo, Gabriele; Quintavalla, Arianna; Pori, Matteo; Giacomini, Daria
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 18 p. 4117 - 4123
反应条件
potassium permanganate; magnesium sulfate in acetone 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 469 - 475
反应条件
chromic acid Yield given;
参考文献
Sharma, Abhishek; Sharma, Naina; Kumar, Rakesh; Sharma, Upendra K.; Sinha, Arun K.
Chemical Communications, 2009 , # 35 p. 5299 - 5301
反应条件
N-iodo-succinimide; water; N-hexadecyl-N,N,N-trimethylammonium bromide in 1,4-dioxane
T=20 - 105°C; 0.333333 h; Microwave irradiation;
参考文献
Sharma, Abhishek; Sharma, Naina; Kumar, Rakesh; Sharma, Upendra K.; Sinha, Arun K.
Chemical Communications, 2009 , # 35 p. 5299 - 5301
反应条件
hydrogen; αα-TREDIP; tris(allyl)rhodium in dichloromethane
48 h; Yield given. Yields of byproduct given;
参考文献
Brown, John M.; Cook, Stephen J.; Khan, Riaz
Tetrahedron, 1986 , vol. 42, # 18 p. 5105 - 5110
反应条件
Ru(IV)(TMP)Cl2; air; sodium hydrogencarbonate in chloroform-d1; water
T=50°C; 7 h;
参考文献
Jiang, Gaoxi; Chen, Jian; Thu, Hung-Yat; Huang, Jie-Sheng; Zhu, Nianyong; Che, Chi-Ming
Angewandte Chemie - International Edition, 2008 , vol. 47, # 35 p. 6638 - 6642
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane
T=-78°C;
参考文献
Shishido, Kozo; Yamashita, Akitake; Hiroya, Kou; Fukumoto, Keiichiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 469 - 475
反应条件
triethylamine in dichloromethane; dimethyl sulfoxide
参考文献
Koch Industries, Inc.
Patent: US5286902 A1, 1994 ;