6-甲氧基-alpha-甲基-2-萘乙醛合成路线 (共 35 条)
反应条件
Sulfolobus solfataricus alcohol dehydrogenase-10; nicotinamide adenine dinucleotide in ethanol
T=80°C; pH=9; 18 h; Inert atmosphereaq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Friest, Jacob A.; Maezato, Yukari; Broussy, Sylvain; Blum, Paul; Berkowitz, David B.
Journal of the American Chemical Society, 2010 , vol. 132, # 17 p. 5930 - 5931
反应条件
ethanol; horse liver alcohol dehydrogenase; NADH dipotassium salt in tetrahydrofuran
pH=8; 24 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Galletti, Paola; Emer, Enrico; Gucciardo, Gabriele; Quintavalla, Arianna; Pori, Matteo; Giacomini, Daria
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 18 p. 4117 - 4123
反应条件
ethanol; horse liver alcohol dehydrogenase; NADH dipotassium salt in acetonitrile
pH=8; 24 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Galletti, Paola; Emer, Enrico; Gucciardo, Gabriele; Quintavalla, Arianna; Pori, Matteo; Giacomini, Daria
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 18 p. 4117 - 4123
反应条件
ethanol; horse liver alcohol dehydrogenase; NADH dipotassium salt
pH=8; 24 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Galletti, Paola; Emer, Enrico; Gucciardo, Gabriele; Quintavalla, Arianna; Pori, Matteo; Giacomini, Daria
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 18 p. 4117 - 4123
反应条件
1: NaHSO3 / methanol; H2O
2: methanol
View Scheme
参考文献
Wuts, Peter G. M.; Bergh, Carol L.
Tetrahedron Letters, 1986 , vol. 27, # 34 p. 3995 - 3998