1-异氰酸-4-(4-异氰酸苯基)苯合成路线 (共 5 条)
反应条件
chlorocatecholborane; triethylamine in toluene 1.) reflux, 5 min, 2.) 0.5 h;
参考文献
Valli, V. L. K.; Alper, H.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 257 - 258
反应条件
1: formaldehyd; aniline With hydrogenchloride in water T=40 - 100°C; 13 h; reflux; 2: phosgene in chlorobenzene T=0 - 210°C; P=2.25023 Torr; 2 h; Heating / reflux; Product distribution / selectivity;
参考文献
Bayer MaterialScience AG
Patent: EP1561746 A2, 2005 ;
Location in patent: Page/Page column 9 ;
反应条件
benzene unter Druck;
参考文献
Snape
Journal of the Chemical Society, 1886 , vol. 49, p. 254
参考文献
Lieser; Nischk
Justus Liebigs Annalen der Chemie, 1950 , vol. 569, p. 59,61
反应条件
T=230 - 250°C; zuletzt bei 310grad;
参考文献
Mashio; Nomachi
Kogyo Kagaku Zasshi, 1952 , vol. 55, p. 266
Chem.Abstr., 1954 , p. 8747