全氟-2,5,8-三甲基-3,6,9-三氧杂十二酰氟合成路线 （共 8 条）
反应条件
potassium fluoride in diethylene glycol dimethyl ether 24 h; Ambient temperature; Further byproducts given;
参考文献
Ishikawa, Nobuo; Sasabe, Mikio
Journal of Fluorine Chemistry, 1984 , vol. 25, p. 241 - 254
反应条件
bis(diethylamino)methane in diethylene glycol dimethyl ether T=-40 - -30°C;
参考文献
Igumnov; Lekontseva; Shipigusev; Mukhametshin
Russian Journal of Applied Chemistry, 2005 , vol. 78, # 3 p. 435 - 437
反应条件
potassium fluoride in diethylene glycol dimethyl ether 24 h; Ambient temperature; Further byproducts given;
参考文献
Ishikawa, Nobuo; Sasabe, Mikio
Journal of Fluorine Chemistry, 1984 , vol. 25, p. 241 - 254
反应条件
potassium fluoride; ethyl fluorooxolate in diethylene glycol dimethyl ether 14 h; Heating; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Paleta, Oldrich; Cirkva, Vladimir; Kvicala, Jaroslav
Journal of Fluorine Chemistry, 1996 , vol. 80, # 2 p. 125 - 134
反应条件
iodine; caesium carbonate in diethylene glycol dimethyl ether T=70°C; 4 h; Yield given;
参考文献
Chen, Grace J.; Chen, Loomis S.; Eapen, Kalathil C.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 1-2 p. 59 - 66
反应条件
potassium fluoride in acetonitrile a.) 1 h, r.t., b) 10 h, 75 deg C; Yields of byproduct given;
参考文献
Chen, L. S.; Eapen, K. C.
Journal of Fluorine Chemistry, 1991 , vol. 55, # 1 p. 93 - 100
反应条件
NiF2; fluorine
T=200°C;
参考文献
Zakharov, V. Yu.; Denisov, A. K.; Novikova, M. D.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 12 p. 1942 - 1945
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 12 p. 1844 - 1846
→
61098-01-9二十八氟-5,8,11,12,15,18-六(三氟甲基)-4,7,10,13,16,19-六氧杂二十二烷
反应条件
T=20°C; Recombination; Decarbonylation; 50 h; Irradiation;
参考文献
Tonelli, Claudio; Tortelli, Vito
Journal of Fluorine Chemistry, 2000 , vol. 101, # 1 p. 117 - 123
