1-乙烯基-1,2,4-三唑合成路线 （共 13 条）
反应条件
mercury(II) diacetate; hydroquinone; trifluoroacetic acid T=70°C; 3 h;
参考文献
Kizhnyaev; Pokatilov; Tsypina; Ratovskii; Vereshchagin; Smirnov
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 7 p. 1056 - 1059
反应条件
sodium hydroxide; tetrabutylammomium bromide in toluene T=60 - 80°C; 24 h;
参考文献
Torres, J.; Lavandera, J. L.; Cabildo, P.; Claramunt, R. M.; Elguero, J.
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 771 - 782
反应条件
potassium hydroxide; acetylene in 1,4-dioxane T=175 - 180°C; P=7600 - 9120 Torr; 1.5 h; Yield given. Yields of byproduct given;
参考文献
Gareev, G. A.; Kirillova, L. P.; Belousov, A. M.; Bukina, N. S.; Vereshchagin, L. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , p. 1494 - 1498
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 8 p. 1751 - 1755
反应条件
tetrabutylammomium bromide; potassium carbonate T=60°C; 48 h;
参考文献
Diez-Barra, Enrique; Hoz, Antonio de la; Sanchez-Migallon, Ana; Tejeda, Juan
Heterocycles, 1992 , vol. 34, # 7 p. 1365 - 1373
反应条件
potassium hydroxide in 1,4-dioxane T=175 - 180°C; P=7600 - 9120 Torr; 1.5 h; Yield given. Yields of byproduct given;
参考文献
Gareev, G. A.; Kirillova, L. P.; Belousov, A. M.; Bukina, N. S.; Vereshchagin, L. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , p. 1494 - 1498
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 8 p. 1751 - 1755
反应条件
potassium hydroxide; water in 1,4-dioxane T=220°C; P=12160 Torr; 16 h; influence of solvent, temperature, catalyst, and reaction time on the yield of the product; other solvents, other temperatures, other catalyst, other reaction time; Product distribution;
参考文献
Ermakova; Tatarova; Kuznetsova
Russian Journal of General Chemistry, 1997 , vol. 67, # 5 p. 805 - 807
反应条件
in water T=350 - 400°C;
参考文献
Attaryan; Baltayan; Sagatelyan; Takmazyan, K. Ts.
Russian Journal of General Chemistry, 2007 , vol. 77, # 12 p. 2176 - 2178
反应条件
potassium hydroxide in 1,4-dioxane T=240°C; 4 h;
参考文献
Trzhtsinskaya, B. V.; Apakina, E. V.; Afonin, A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 4.2 p. 834 - 836
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 4 p. 928 - 931
反应条件
tetrabutyl ammonium fluoride; iron(III) chloride; copper T=50°C; 24 h;
参考文献
Song, Ren-Jie; Deng, Chen-Liang; Xie, Ye-Xiang; Li, Jin-Heng
Tetrahedron Letters, 2007 , vol. 48, # 44 p. 7845 - 7848
反应条件
mercury(II) diacetate T=95 - 100°C; 2 h;
参考文献
Gareev, G. A.; Kirillova, L. P.; Belousov, A. M.; Bukina, N. S.; Vereshchagin, L. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , p. 1494 - 1498
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 8 p. 1751 - 1755
