反应条件
in dichloromethane N2 atmosphere, addn. of soln. of stannyl compound to suspension of Me2SnBr2 at room temp., addn. of soln. of tBuBBr2 at -68 to -40°C (130min), warming to room temp.; removement of solvent (25°C, 12 Torr), condensation of Me3SnBr and Me2SnBr2 into a trap (-78°C, 4 h), fractional distillation (69-77°C, 1E-5 Torr); elem. anal.;
参考文献
Diemer, Stefan; Noeth, Heinrich; Storch, Wolfgang
European Journal of Inorganic Chemistry, 1999 , # 9 p. 1765 - 1780
