(1S)-(+)-樟脑醌合成路线 (共 24 条)
反应条件
2C24BF20(1-)*Ca(2+); dihydrogen peroxide; oxalic acid in water; 1,2-dichloro-ethane T=50°C; 18 h; Reagent/catalyst;
参考文献
NATIONAL UNIVERSITY CORPORATION NAGOYA UNIVERSITY; Ishihara, Kazuaki; Uyanik, Muhammet
Patent: US2013/217898 A1, 2013 ;
Location in patent: Paragraph 0070; 0074; 0090 ;
反应条件
selenium(IV) oxide in ethanol T=150°C; 1.25 h; microwave irradiation;
参考文献
Belsey, Sarah; Danks, Timothy N.; Wagner, Gabriele
Synthetic Communications, 2006 , vol. 36, # 8 p. 1019 - 1024
反应条件
SeO2 in acetic anhydride
参考文献
Florida State University
Patent: US6111144 A1, 2000 ;
反应条件
1: With sodium carbonate in dimethyl sulfoxide T=20°C; 2: With tetra-(n-butyl)ammonium iodide T=20 - 90°C; 48.5 h;
参考文献
Kannappan, Jayaraman; Bedekar, Ashutosh V.
Journal of Chemical Research, 2012 , vol. 36, # 3 p. 141 - 143
反应条件
hydrogenchloride; water in 1,4-dioxane Heating;
参考文献
Theis, W.; Bethaeuser, W.; Regitz, M.
Tetrahedron, 1985 , vol. 41, # 10 p. 1965 - 1972
反应条件
hydrogenchloride; formaldehyd Hydrolysis; Heating;
参考文献
Love, Brian E.; Jones, Edward G.
Synthetic Communications, 1999 , vol. 29, # 16 p. 2831 - 2840
反应条件
selenium(IV) oxide in water T=150°C; 1.25 h; microwave irradiation; Further byproducts given;
参考文献
Belsey, Sarah; Danks, Timothy N.; Wagner, Gabriele
Synthetic Communications, 2006 , vol. 36, # 8 p. 1019 - 1024
反应条件
benzeneseleninic anhydride in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Cussans, Nigel J.; Ley, Steven V.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1650 - 1653
反应条件
hydrogen bromide in acetic acid T=60°C; 5 h;
参考文献
Ellis, Martin K.; Golding, Bernard T.; Watson, William P.
Journal of the Chemical Society, Chemical Communications, 1984 , # 23 p. 1600 - 1602
反应条件
1: 81 percent / CH2Cl2 / Ambient temperature 2: 78 percent / H2O, 7M HCl / dioxane / Heating View Scheme
参考文献
Theis, W.; Bethaeuser, W.; Regitz, M.
Tetrahedron, 1985 , vol. 41, # 10 p. 1965 - 1972