(1S)-(+)-樟脑醌合成路线 (共 24 条)
反应条件
selenium(IV) oxide; acetic anhydride T=140 - 150°C;
参考文献
Chakravarti
Journal of the Indian Chemical Society, 1943 , vol. 20, p. 301,304
Journal of the Chemical Society, 1947 , p. 1565,1568
反应条件
1: 9.4 percent / toluene p-sulphonic acid / benzene / 18 h / Heating 2: 48percent HBr / acetic acid / 5 h / 60 °C View Scheme
参考文献
Ellis, Martin K.; Golding, Bernard T.; Watson, William P.
Journal of the Chemical Society, Chemical Communications, 1984 , # 23 p. 1600 - 1602
反应条件
sodium hydrogensulfite; acetic acid <d-camphor>-quinone;
参考文献
Gluud
Chemische Berichte, 1915 , vol. 48, p. 426,430
Chem. Zentralbl., 1915 , vol. 86, # II p. 861
反应条件
in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Cussans, Nigel J.; Ley, Steven V.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1650 - 1653
反应条件
1: m-chloroperbenzoic acid 2: Ambient temperature View Scheme
参考文献
Cussans, Nigel J.; Ley, Steven V.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1650 - 1653
反应条件
Ambient temperature;
参考文献
Cussans, Nigel J.; Ley, Steven V.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1650 - 1653
反应条件
sodium percarbonate in water; acetone T=65°C; 0.166667 h; other α-diketones, var. time;
参考文献
Yang; Evans; Yamazaki; Narayanna; Kabalka
Synthetic Communications, 1993 , vol. 23, # 8 p. 1183 - 1187
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Wulfman,D.S. et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1975 , p. 522 - 529
反应条件
1: 24 percent / PTSA / benzene / Heating 2: HBA / 3 h / 65 °C View Scheme
参考文献
Ellis, Martin K.; Golding, Bernard T.; Maude, Antony B.; Watson, William P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 4 p. 747 - 755
反应条件
sulfuric acid 1. ether, MeOH, 48h, room temperature, 2. reflux, 3h; Yield given. Multistep reaction;
参考文献
Shitole, H.R.; Nayak, U.R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 5 p. 415 - 417