1,1-二(4-氯苯基)-2,2-二氯乙醇合成路线 (共 7 条)
反应条件
sodium hydroxide; sodium tetrahydroborate in ethanol -> 28 deg C (10 min.), 10 min.;
参考文献
McDonald, Richard N.; Cousins, Raymond C.
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 2976 - 2984
反应条件
1: 99 percent / chlorine / acetic acid / 0.92 h / 51 - 58 °C 2: 98 percent / NaBH4, aqueous NaOH / ethanol / -> 28 deg C (10 min.), 10 min. View Scheme
参考文献
Kedziora, Kinga; Bisogno, Fabricio R.; Lavandera, Ivan; Gotor-Fernandez, Vicente; Montejo-Bernardo, Jose; Garcia-Granda, Santiago; Kroutil, Wolfgang; Gotor, Vicente
ChemCatChem, 2014 , vol. 6, # 4 p. 1066 - 1072
反应条件
aluminium amalgam; isopropyl alcohol
参考文献
Bal'on,Ya.G.; Shul'man,M.D.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 9 p. 1973 - 1979,1926 - 1931
参考文献
Bal'on,Ya.G.; Shul'man,M.D.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 9 p. 1973 - 1979,1926 - 1931
反应条件
sulfuric acid; boron trifluoride
参考文献
Counsell; Willette; DiGuilio
Journal of medicinal chemistry, 1967 , vol. 10, # 5 p. 975 - 977
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen in tert-butyl methyl ether
T=20°C; P=760.051 Torr; 24 h; Enzymatic reaction;
参考文献
Kedziora, Kinga; Diaz-Rodriguez, Alba; Lavandera, Ivan; Gotor-Fernandez, Vicente; Gotor, Vicente
Green Chemistry, 2014 , vol. 16, # 5 p. 2448 - 2453
反应条件
sulfuric acid; sulfur trioxide
参考文献
Bal'on,Ya.G.; Shul'man,M.D.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 9 p. 1973 - 1979,1926 - 1931