3-(1-甲基-1H-吡咯-2-基)-丙烯酸乙酯合成路线 (共 2 条)
反应条件
potassium phosphate; Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); tetrabutylammomium bromide in water; N,N-dimethyl-formamide T=100°C; Heck coupling; 8 h; optical yield given as percent destereoselective reaction;
参考文献
Lee, Dong-Hwan; Taher, Abu; Hossain, Shahin; Jin, Myung-Jong
Organic Letters, 2011 , vol. 13, # 20 p. 5540 - 5543
反应条件
water; barium dihydroxide in 1,4-dioxane T=70°C; 2 h;
参考文献
Sinisterra, J. V.; Mouloungui, Z.; Delmas, M.; Gaset, A.
Synthesis, 1985 , # 12 p. 1097 - 1100