2-溴-3-甲氧基丙酸甲酯合成路线 （共 9 条）
反应条件
mercury(II) diacetate
参考文献
SYNGENTA LIMITED
Patent: WO2004/48316 A1, 2004 ;
Location in patent: Page 38-39 ;
反应条件
methanol; mercury(II) diacetate Umsetzen mit KBr in Wasser und Einw. von Brom auf das anstandene Produkt in Chloroform im Sonnenlicht unterhalb 55grad;
参考文献
Shell Oil Company
Patent: US4439226 A1, 1984 ;
反应条件
N-bromosuccinmide; sulfuric acid
参考文献
Heasley, Victor L.; Wade, Kimberley E.; Aucoin, Thomas G.; Gipe, Daphne E.; Shellhamer Dale F.; Heasley, Gene E.
Journal of Organic Chemistry, 1983 , vol. 48, # 8 p. 1377 - 1379
反应条件
methyl hypobromite; boron trifluoride diethyl etherate in dichloromethane T=25°C; 0.0833333 h; Yield given;
参考文献
Heasley, Victor L.; Gipe, Robert K.; Martin, Jody L.; Wiese, Harry C.; Oakes, Melanie L.; Shellhamer, Dale F.
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3195 - 3199
反应条件
boron trifluoride diethyl etherate in dichloromethane T=25°C; 0.0833333 h; Yield given;
参考文献
Heasley, Victor L.; Gipe, Robert K.; Martin, Jody L.; Wiese, Harry C.; Oakes, Melanie L.; Shellhamer, Dale F.
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3195 - 3199
反应条件
sodium 0 degC, 1 h then r.t., 2 h;
参考文献
Effenberger, Franz; Zoller, Gerhard
Tetrahedron, 1988 , vol. 44, # 17 p. 5573 - 5582
反应条件
mercury(II) diacetate; bromine; potassium bromide Multistep reaction;
参考文献
Beguin, Cecile; LeTiran, Arnaud; Stables, James P.; Voyksner, Robert D.; Kohn, Harold
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 11 p. 3079 - 3096
反应条件
sodium methylate in methanol
参考文献
Joucla, Marc; Fouchet, Bernard; le Brun, Jacques; Hamelin, Jack
Tetrahedron Letters, 1985 , vol. 26, # 9 p. 1221 - 1224
参考文献
SYNGENTA LIMITED
Patent: WO2004/47538 A1, 2004 ;
Location in patent: Page 53 ;
