1,5-双(二苯基膦)戊烷合成路线 (共 3 条)
反应条件
1: lithium; triphenylphosphine in tetrahydrofuran T=50°C; Inert atmosphere; 2: 1,5-dichloro-pentane in tetrahydrofuran T=0 - 80°C; Inert atmosphere;
参考文献
Shatunov; Korlyukov; Lebedev; Sheludyakov; Kozyrkin; Orlov, V.Yu.
Journal of Organometallic Chemistry, 2011 , vol. 696, # 10 p. 2238 - 2251
反应条件
cesium hydroxide; 4 Angstroem MS in N,N-dimethyl-formamide T=23°C; 72 h;
参考文献
Honaker, Matthew T.; Salvatore, Ralph Nicholas
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 2 p. 277 - 283
反应条件
lithium in tetrahydrofuran
参考文献
Brooks, Peter; Craig, Donald C.; Gallagher, Michael J.; Rae, A. David; Sarrof, Adrien
Journal of Organometallic Chemistry, 1987 , vol. 323, p. C1 - C4