反应条件
1: 97 percent / Ph3P*Br2, pyridine / CCl4; CH2Cl2 / Ambient temperature 2: 1.) NaNH2, DMPU / 1.) THF, 2 h, 2.) THF, -from -10 deg C to RT, 10 h 3: 1.) NaNH2, DMPU / 1.) THF, 2 h, 2.) THF, -from -10 deg C to RT, overnight 4: aq. PTSA / methanol / 0.75 h / Heating 5: 99 percent / LiAlH4 / tetrahydrofuran / Ambient temperature 6: 98 percent / H2, quinoline / Pd/BaSO4 / hexane / 4 h / Ambient temperature View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 34, # 6 p. 531 - 534
