反应条件
1: 11-hydroxyundecyne With n-butyllithium in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; Petroleum ether
T=-78 - -30°C;
2: n-bromopentane in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane
T=20°C; 12 h;
参考文献
Ohashi, Kazuyoshi; Winarno, Hendig; Mukai, Mutsuko; Shibuya, Hirotaka
Chemical and pharmaceutical bulletin, 2003 , vol. 51, # 4 p. 463 - 466
