(2E)-4-甲基-2-硝基-2-戊烯合成路线 (共 5 条)
反应条件
1: With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in ethylene glycol dimethyl ether T=20°C; 0.166667 h; Inert atmosphere; 2: With tetrabutylammomium bromide; sodium nitrite in ethylene glycol dimethyl ether 5 h; Reflux;
参考文献
Chang, Meng-Yang; Lin, Chung-Han; Tai, Hang-Yi
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3194 - 3198
反应条件
phenolformaldehyde-based ethylenediamine-modified polymer T=90°C; Henry reaction; 6 h;
参考文献
Yan, Shaoyu; Gao, Yuan; Xing, Rong; Shen, Yali; Liu, Yueming; Wu, Peng; Wu, Haihong
Tetrahedron, 2008 , vol. 64, # 27 p. 6294 - 6299
反应条件
phthalic anhydride T=180°C; P=30 Torr;
参考文献
Wang, Liang; Li, Pengfei; Menche, Dirk
Angewandte Chemie - International Edition, 2010 , vol. 49, # 48 p. 9270 - 9273
反应条件
1.1: caesium carbonate / ethylene glycol dimethyl ether / 5 h / 20 °C / |Inert atmosphere 2.1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl / ethylene glycol dimethyl ether / 0.17 h / 20 °C / |Inert atmosphere 2.2: 5 h / |Reflux View Scheme
参考文献
Chang, Meng-Yang; Lin, Chung-Han; Tai, Hang-Yi
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3194 - 3198
反应条件
sodium carbonate; benzene
参考文献
Sanno
Yakugaku Zasshi, 1958 , vol. 78, p. 1119,1122
Chem.Abstr., 1959 , p. 5239