in benzene
BCl3 is introduced into boiling soln. of (2-CH3-C6H4)HgCl, boiling under reflux for 4 h, (cooler at -78°C,) excess of BCl3 escapes, HgCl2 removed; distn., ratio of obtained isomers ortho:meta=l9:1, pure ortho compound by repeated distn.;
参考文献
Eggers; Kettle
Inorganic Chemistry, 1967 , vol. 6, p. 1975
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Gmelin Handbook: B: B-Verb.9, 5.2.6, page 205 - 215
Gerrard, W.; Howarth, M.; Mooney, E. F.; Pratt, D. E.
Journal of the Chemical Society, 1963 , p. 1582 - 1584
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Gmelin Handbook: B: B-Verb.9, 5.2.6, page 205 - 215
