反应条件
1: 1.) ethylmagnesium bromide, 2.) copper(I) cyanide / 1.) tetrahydrofuran, 20 deg C, 2 h, 2.) reflux, 24 h 2: diethyl ether 3: hydrogen / Lindlar catalyst / ethyl acetate 4: hydrogen / 10percent palladium on carbon / ethyl acetate View Scheme
参考文献
Frankel, Edwin N.; Garwood, Robert F.; Khambay, Bhupinder P. S.; Moss, Gerard P.; Weedon, Basil C. L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2233 - 2240