反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere 1.2: 2 h / -78 °C / Inert atmosphere 1.3: -78 - 20 °C / Saturated solution 2.1: Pd(OH)2/C (6 w/w); hydrogen / methanol / 24 h / 20 °C / 3800.26 Torr 3.1: hydrogenchloride; water / 6 h / Reflux 3.2: Dowex 50WX8-100 View Scheme
参考文献
Davies, Stephen G.; Fletcher, Ai M.; Lv, Linlu; Roberts, Paul M.; Thomson, James E.
Tetrahedron Asymmetry, 2012 , vol. 23, # 11-12 p. 910 - 925
