4-(1-羟基-2-丙炔-1-基)苯甲醛合成路线 （共 5 条）
反应条件
sulfuric acid; silica gel in dichloromethane T=20°C; Hydrolysis;
参考文献
Ulrich, Karine; Porhiel, Emmanuel; Peron, Vincent; Ferrand, Vincent; Le Bozec, Hubert
Journal of Organometallic Chemistry, 2000 , vol. 601, # 1 p. 78 - 86
反应条件
copper(l) chloride in acetonitrile T=60°C; 15 h; Inert atmosphere;
参考文献
Kolarovic, Andrej; Faberova, Zuzana
Journal of Organic Chemistry, 2009 , vol. 74, # 18 p. 7199 - 7202
反应条件
1: 75 percent / nBuLi / tetrahydrofuran 2: 85 percent / H2SO4; SiO2 / CH2Cl2 / 20 °C View Scheme
参考文献
Ulrich, Karine; Porhiel, Emmanuel; Peron, Vincent; Ferrand, Vincent; Le Bozec, Hubert
Journal of Organometallic Chemistry, 2000 , vol. 601, # 1 p. 78 - 86
反应条件
1.1: n-butyllithium / tetrahydrofuran / 1.5 h / -78 °C / |Inert atmosphere 1.2: 1.5 h / -78 - 20 °C / |Inert atmosphere 2.1: potassium carbonate / methanol / 20 °C / |Inert atmosphere View Scheme
参考文献
Bhanuchandra; Kuram, Malleswara Rao; Sahoo, Akhila K.
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 11824 - 11834
参考文献
Tokunaga, Yuji; Ohta, Go; Yamauchi, Yuji; Goda, Tatsuhiro; Kawai, Nobuhiko; Sugihara, Takumichi; Shimomura, Youji
Chemistry Letters, 2006 , vol. 35, # 7 p. 766 - 767
