反应条件
1: 2.) 2,6-di-tert-butylphenol / 1.) toluene, -78 deg C, 2.) THF, -78 deg C to room temperature, 30 min 2: 75 percent / 1.) H2, 2.) HCl / 1.) Pd-C / 1.) AcOH, 50 deg C, 4 bar, 2.) MeOH 3: 95 percent / TFA / 16 h / Ambient temperature View Scheme
参考文献
Davies, Stephen G.; Ichihara, Osamu; Lenoir, Isabelle; Walters, Iain A. S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 11 p. 1411 - 1416