3-(4-叔丁基苯基)-1-丙烯合成路线 (共 22 条)
反应条件
cesium fluoride; palladium diacetate in 1,4-dioxane T=100°C; Stille cross-coupling; 4 h;
参考文献
Gajare, Anil S.; Jensen, Rader S.; Toyota, Kozo; Yoshifuji, Masaaki; Ozawa, Fumiyuki
Synlett, 2005 , # 1 art. no. U25204ST, p. 144 - 148
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in ethylene glycol dimethyl ether T=85°C; 9 h; Inert atmosphere;
参考文献
Denmark, Scott E.; Werner, Nathan S.
Journal of the American Chemical Society, 2008 , vol. 130, # 48 p. 16382 - 16393
反应条件
indium(III) chloride; indium; lithium chloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=100°C; 6 h;
参考文献
Seomoon, Dong; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 3 p. 1165 - 1168
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in toluene T=110°C; Suzuki-Miyaura coupling; 15 h; Inert atmosphere;
参考文献
Gerbino, Dario C.; Mandolesi, Sandra D.; Schmalz, Hans-Guenther; Podesta, Julio C.
European Journal of Organic Chemistry, 2009 , # 23 p. 3964 - 3972
反应条件
palladium diacetate in 1,4-dioxane T=100°C; Suzuki-Miyaura coupling; 6 h;
参考文献
Gerbino, Dario C.; Mandolesi, Sandra D.; Schmalz, Hans-Guenther; Podesta, Julio C.
European Journal of Organic Chemistry, 2009 , # 23 p. 3964 - 3972
反应条件
1: 1-bromo-4-(1,1-dimethylethyl)benzene With iodine; magnesium in diethyl ether 2 h; Inert atmosphere; 2: allyl bromide in diethyl ether T=0°C; 0.75 h; Inert atmosphere;
参考文献
Wang, Xi; Ye, Yuxuan; Zhang, Songnan; Feng, Jiajie; Xu, Yan; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2011 , vol. 133, # 41 p. 16410 - 16413
反应条件
xanthone powder in acetonitrile T=20°C; Photolysis;
参考文献
Milanesi, Silvia; Fagnoni, Maurizio; Albini, Angeld
Journal of Organic Chemistry, 2005 , vol. 70, # 2 p. 603 - 610
反应条件
tert.-butylnitrite in acetonitrile T=45 - 50°C; 1.33 h;
参考文献
Ek, Fredrik; Axelsson, Oskar; Wistrand, Lars-Goeran; Frejd, Torbjoern
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6376 - 6381
参考文献
Uniroyal Chemical Company, Inc.; Uniroyal Chemical Ltd./Ltee
Patent: US5486533 A1, 1996 ;
反应条件
caesium carbonate in water; acetonitrile 18 h; Inert atmosphereUV-irradiation;
参考文献
Qrareya, Hisham; Raviola, Carlotta; Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 6016 - 6024