甲基3-(3’,4’-二甲氧基苯基)丙酸酯合成路线 （共 17 条）
反应条件
formic acid; sodium sulfate; triethylamine in methanol; chloroform; Petroleum ether
参考文献
BIOGAL GYOGYSZERGYAR
Patent: EP578850 A1, 1994 ;
反应条件
ammonium formate; silica gel; palladium dichloride in formic acid; water 0.1 h; microwave irradiation;
参考文献
Kumar, Vinod; Sharma, Anuj; Sinha, Arun K.
Helvetica Chimica Acta, 2006 , vol. 89, # 3 p. 483 - 495
反应条件
hydrogen; palladium on activated charcoal in methanol P=760 Torr; 0.5 h; Ambient temperature;
参考文献
Lam, Thi Bach Tuyet; Iiyama, Kenji; Stone, Bruce A.
Phytochemistry (Elsevier), 1992 , vol. 31, # 4 p. 1179 - 1184
反应条件
1: aq. HCl / 6 h / Heating 2: H2 / 10percent Pd/C / methanol / 0.5 h / 760 Torr / Ambient temperature View Scheme
参考文献
Lam, Thi Bach Tuyet; Iiyama, Kenji; Stone, Bruce A.
Phytochemistry (Elsevier), 1992 , vol. 31, # 4 p. 1179 - 1184
参考文献
Chemex Pharmaceuticals, Inc.
Patent: US4954659 A1, 1990 ;
反应条件
potassium carbonate in acetone T=70°C; 6 h;
参考文献
Yang, Jian; Yang, Jing Xiang; Zhang, Fang; Chen, Gang; Pan, Wei; Yu, Rui; Wu, Shuwen; Tien, Po
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 12 p. 2680 - 2684
反应条件
sodium hydride in tetrahydrofuran
参考文献
Bohman; Nordlander; Nordenhem; Sunnerheim; Borg-Karlson; Unelius
Journal of Chemical Ecology, 2008 , vol. 34, # 3 p. 339 - 352
反应条件
tetra-(n-butyl)ammonium iodide; potassium carbonate in acetone
参考文献
Koufaki, Maria; Kiziridi, Christina; Nikoloudaki, Faidra; Alexis, Michael N.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 15 p. 4223 - 4227
反应条件
1: sodium 2: amalgamated aluminium; diethyl ether View Scheme
参考文献
Kindler; Peschke
Archiv der Pharmazie (Weinheim, Germany), 1932 , vol. 270, p. 353,359
参考文献
Rassadin, Valentin A.; Six, Yvan
Tetrahedron, 2014 , vol. 70, # 4 p. 787 - 794
