5-甲氧基-1H-苯并噻唑合成路线 （共 5 条）
反应条件
1: With tert.-butylnitrite in acetonitrile T=0 - 25°C; 2: With sodium hydrogencarbonate in water
参考文献
AVENTIS AGRICULTURE; MERIAL LIMITED; Soll, Mark David; Le Hir de Fallois, Loic Patrick; Huber, Scot Kevin; Lee, Hyoung Ik; Wilkinson, Douglas Edward; Jacobs, Robert Toms
Patent: US2014/80862 A1, 2014 ;
Location in patent: Paragraph 0552 ;
反应条件
acetic acid; sodium nitrite in water T=4 - 50°C;
参考文献
Patel, Pallav D.; Patel, Maulik R.; Kocsis, Bela; Kocsis, Erika; Graham, Steven M.; Warren, Andrew R.; Nicholson, Stacia M.; Billack, Blase; Fronczek, Frank R.; Talele, Tanaji T.
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 6 p. 2214 - 2222
反应条件
acetic acid; sodium nitrite in water T=4 - 70°C; stereoselective reaction;
参考文献
Zhou, Wang; Yang, Youqing; Wang, Zhiwei; Deng, Guo-Jun
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 2 p. 251 - 254
参考文献
Fel'dman; Usowskaja
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 1699,1701
Chem.Abstr., 1949 , p. 2618
反应条件
1: NaNO2; aqueous HCl 2: aqueous acetic acid View Scheme
参考文献
Fel'dman; Usowskaja
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 1699,1701
Chem.Abstr., 1949 , p. 2618
