magnesium in diethyl ether

sodium periodate; ruthenium trichloride in tetrachloromethane; acetonitrile T=20°C; 24 h;

hydrogen cation in diethyl ether T=5°C; 1 h;

1: 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodooctane With magnesium in diethyl ether Grignard reaction; 4 h; Inert atmosphere; 2: carbon dioxide in diethyl ether T=0°C; Grignard reaction; Inert atmosphere; 3: With sulfuric acid in diethyl ether Grignard reaction; Inert atmosphere;

1: Bu3SnH / 20 °C 2: aq. NaIO4 / RuCl3*3H2O / CCl4; acetonitrile / 24 h / 20 °C View Scheme

1: Mg / CH3I / diethyl ether / 10 h / 20 °C 2: 2.) H(1+) / diethyl ether / 1 h / 5 °C View Scheme

N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C;