3-甲基-2(3H)-苯并噻唑酮合成路线 （共 74 条）
反应条件
hydrogenchloride in chloroform-d1
T=25°C; 2 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
sodium hydroxide
2 h; Ambient temperature;
参考文献
Diouf; Depreux; Lesieur; Poupaert; Caignard
European Journal of Medicinal Chemistry, 1995 , vol. 30, # 9 p. 715 - 719
反应条件
copper(ll) bromide
T=120°C; 15 h; Reagent/catalyst;
参考文献
Yang, Yuan; Zhang, Xiaoyun; Zeng, Weilan; Huang, Hui; Liang, Yun
RSC Advances, 2014 , vol. 4, # 12 p. 6090 - 6093
反应条件
1: SO2Cl2 / CDCl3 / 0.17 h / 5 °C
2: 92 percent / CDCl3 / 24 h / 25 °C
View Scheme
参考文献
Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 1986 , vol. 51, # 10 p. 1866 - 1881
反应条件
N(Et)4ClO4 in acetonitrile
2 h; Ambient temperaturein 0,1 M (C2H5)4NClO4;
参考文献
Itoh, Takashi; Nagata, Kazuhiro; Okada, Mamiko; Ohsawa, Akio
Tetrahedron, 1993 , vol. 49, # 22 p. 4859 - 4870
参考文献
Hoechst Aktiengesellschaft
Patent: US4429134 A1, 1984 ;
反应条件
sulfuric acid; water in chloroform-d1
T=55°C; 192 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
sulfuryl dichloride in chloroform-d1
T=25°C; 72 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
1: 84 percent / CHCl3 / 70 h / 25 °C
2: SO2Cl2 / CDCl3 / 0.17 h / 5 °C
3: 92 percent / CDCl3 / 24 h / 25 °C
View Scheme
参考文献
Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 1986 , vol. 51, # 10 p. 1866 - 1881
反应条件
sulfuryl dichloride in chloroform-d1
T=25°C; 72 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
