3-甲基-2(3H)-苯并噻唑酮合成路线 （共 74 条）
反应条件
1: 81 percent / K2CO3 / butan-2-one / Heating
2: 77 percent Chromat. / 48percent HBr, PhOH / 5.5 h / Heating
View Scheme
参考文献
Mellor, Michael; Osbourn, Susan E.
Tetrahedron, 1991 , vol. 47, # 12-13 p. 2255 - 2262
反应条件
1.1: sulfuryl dichloride / chloroform-d1 / 25 °C
1.2: 2 h
2.1: hydrogenchloride / chloroform-d1 / 2 h / 25 °C
View Scheme
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
1: O-isopropyl N-methyl-N-phenylthiocarbamate With sulfuryl dichloride in chloroform-d1
T=25°C;
2: in chloroform-d1; methanol-d4
2 h;
3: N-methylaniline in chloroform-d1; methanol-d4
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
ethanol; triethylamine
参考文献
Van Dormael; Ghys
Bulletin des Societes Chimiques Belges, 1948 , vol. 57, p. 24,29
反应条件
oxirane in acetic acid
参考文献
Sohar,P. et al.
Journal of Heterocyclic Chemistry, 1968 , vol. 5, p. 769 - 771
反应条件
diphenyldiazo-methane in dichloromethane
Heating;
参考文献
Akiba,K. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, # 7 p. 1913 - 1916
反应条件
1.) CHCl3, 0 to 10 deg C, 4 h, 2.) 25 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Barany, George; Schroll, Alayne L.; Mott, Andrew W.; Halsrud, David A.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4750 - 4761
反应条件
1: DBU / dimethylformamide
2: (i) O2, O3, CHCl3, (ii) diazoethane, Et2O, (iii) aq. EtOH
View Scheme
参考文献
Takamizawa; Matsushita; Harada
Chemical and Pharmaceutical Bulletin, 1977 , vol. 25, # 5 p. 991 - 1000
反应条件
lithium borohydride in diethyl ether
参考文献
Zinner,H.; Nimmich,W.
Journal fuer Praktische Chemie (Leipzig), 1961 , vol. 14, p. 139 - 149
反应条件
2-phenyl-ethanol; benzoic acid; diethylazodicarboxylate in tetrahydrofuran
96 h; Ambient temperaturevar. temp. and time; add of N,N-dimethylaniline as cat; var. reag.: butanol, 2-octanol, t-BuOH; Product distribution;
参考文献
Mitsunobu, Oyo; Takemasa, Akira; Endo, Ryosuke
Chemistry Letters, 1984 , p. 855 - 858
