3-甲基-2(3H)-苯并噻唑酮合成路线 （共 74 条）
反应条件
1: SOCl2 / 45 °C
2: LiBH4 / diethyl ether
View Scheme
参考文献
Zinner,H.; Nimmich,W.
Journal fuer Praktische Chemie (Leipzig), 1961 , vol. 14, p. 139 - 149
反应条件
1: chloroform-d1 / 24 h / 4 - 25 °C
2: sulfuryl dichloride / chloroform-d1 / 25 °C
View Scheme
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
in chloroform-d1
T=25°C;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
参考文献
Kohn,H. et al.
Journal of Organic Chemistry, 1978 , vol. 43, p. 4961 - 4965
反应条件
in chloroform-d1
T=25°C; 48 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
in chloroform-d1
T=25°C; 72 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
in chloroform-d1
T=25°C; 72 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
in chloroform-d1
T=4 - 25°C; 1 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
1: O-methyl N-methyl-N-phenylcarbamothioate; (chlorocarbonyl)sulfenyl chloride in chloroform-d1
T=25°C;
2: N-methylaniline in chloroform-d1
72 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
hydrogen bromide; phenol
5.5 h; Heating;
参考文献
Mellor, Michael; Osbourn, Susan E.
Tetrahedron, 1991 , vol. 47, # 12-13 p. 2255 - 2262
