N-(4-甲氧基苯基)-4-甲氧基苯甲酰胺合成路线 (共 18 条)
反应条件
1: thionyl chloride; N,N-dimethyl-formamide / 0.5 h / Inert atmosphere 2: 3 h / 120 °C View Scheme
参考文献
Robertson, Jeffrey M.; Contreras, Cristina G.; Bates, Robert B.; Hall
Macromolecules, 2011 , vol. 44, # 14 p. 5586 - 5589
参考文献
Robertson, Jeffrey M.; Contreras, Cristina G.; Bates, Robert B.; Hall
Macromolecules, 2011 , vol. 44, # 14 p. 5586 - 5589
参考文献
Chapman; Fidler
Journal of the Chemical Society, 1936 , p. 448,451
反应条件
in methanol T=25°C; ΔH(excit.), ΔS(excit.); KineticsProduct distributionThermodynamic data;
参考文献
Lee, Byung Choon; Yoon, Ji Hyun; Lee, Cheal Gyu; Lee, Ikchoon
Journal of Physical Organic Chemistry, 1994 , vol. 7, # 6 p. 273 - 279
反应条件
in chlorobenzene; tert-butyl alcohol T=25°C; other concentration of tert-butyl alcohole; Rate constant;
参考文献
Shpan'ko, I. V.; Likhomanenko, E. E.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 9 p. 1702 - 1710
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 9 p. 1896 - 1904
反应条件
1: phosphorus (V)-chloride / 75 °C
2: diethyl ether / 80 - 90 °C
3: aqueous KOH
4: Erhitzen im Hochvakuum
View Scheme
参考文献
Seka; Fuchs
Monatshefte fuer Chemie, 1931 , vol. 57, p. 52,58
反应条件
Lawesson's reagent in chlorobenzene
3 h; Heating;
参考文献
Stevens, Malcolm F. G.; McCall, Carol J.; Lelieveld, Peter; Alexander, Peter; Richter, Audrey; Davies, Donna E.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 11 p. 1689 - 1695
反应条件
1: 50 percent / phosphorpentasulphide / CH2Cl2 / 6 h / Heating
2: hydrazine hydrate / toluene / 1 h / Heating
View Scheme
参考文献
Clemence; Joliveau-Maushart; Meier; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 3 p. 257 - 266