(3Z)-3-甲基戊-1,3-二烯合成路线 (共 8 条)
反应条件
tri-isobutyl aluminium; Ni(mesal)2 in pentane
T=25°C; 15 h;
参考文献
Caporusso, Anna Maria; Giacomelly, Giampaolo; Lardicci, Luciano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1900 - 1908
反应条件
manganese(II) 2,4-pentanedionate in pentane
T=25°C; 10 h;
参考文献
Caporusso, Anna Maria; Giacomelly, Giampaolo; Lardicci, Luciano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1900 - 1908
反应条件
tri-isobutyl aluminium in pentane
T=25°C; 40 h;
参考文献
Caporusso, Anna Maria; Giacomelly, Giampaolo; Lardicci, Luciano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1900 - 1908
反应条件
toluene-4-sulfonic acid
参考文献
Bartlett,P.D. et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 2049 - 2056
反应条件
in pentane
T=25°C; 40 h;
参考文献
Caporusso, Anna Maria; Giacomelly, Giampaolo; Lardicci, Luciano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1900 - 1908
反应条件
hydrogen bromide in water
Dehydration; Heating; Title compound not separated from byproducts;
参考文献
Viktorov; Zubritskii
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 12 p. 1755 - 1765
反应条件
tetrabutyl ammonium fluoride
参考文献
Nativi, Cristina; Taddei, Maurizio; Mann, Andre
Tetrahedron, 1989 , vol. 45, # 4 p. 1131 - 1144
反应条件
in gas
T=299.9°C; Heatingother temperature; Thermodynamic dataRate constantKinetics;
参考文献
Scherzer, K.; Claus, P.; Karwath, M.
Zeitschrift fuer Physikalische Chemie (Leipzig), 1985 , vol. 266, # 2 p. 321 - 328