(S)-(-)-乳酸甲酯合成路线 (共 55 条)
反应条件
carbon dioxide T=165°C; P=14711.4 - 44428.6 Torr; 1 h; Industry scale; Product distribution / selectivity;
参考文献
Fliedel, Christophe; Vila-Vicosa, Diogo; Calhorda, Maria Jose; Dagorne, Samuel; Aviles, Teresa
ChemCatChem, 2014 , vol. 6, # 5 p. 1357 - 1367
反应条件
carbon dioxide T=165°C; P=21110.9 - 39353.1 Torr; 1 h; Industry scale; Product distribution / selectivity;
参考文献
COUNCIL OF SCIENTIFIC and INDUSTRIAL RESEARCH; BARVE, Prashant, Purushottam; KULKARNI, Bhaskar, Dattatraya; GUPTE, Milind, Yashwant; NENE, Sanjay, Narayan; SHINDE, Ravindra, William
Patent: WO2011/27211 A2, 2011 ;
Location in patent: Page/Page column 12-13 ;
反应条件
tris(N,N-dimethylamino)methane in THF-d8 (tetrahydrofuran-d8) T=25°C;
参考文献
Csihony, Szilard; Beaudette, Tristan T.; Sentman, Alan C.; Nyce, Gregory W.; Waymouth, Robert M.; Hedrick, James L.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 9-10 p. 1081 - 1086
反应条件
indium; iodine transesterification; 7 h; Heating;
参考文献
Ranu, Brindaban C.; Dutta, Pinak; Sarkar, Arunkanti
Journal of Organic Chemistry, 1998 , vol. 63, # 17 p. 6027 - 6028
反应条件
immobilized lipase B from Candida antarctica in tert-butyl methyl ether T=65°C; 4 h; Resolution of racemateEnzymatic reaction; Temperature; enantioselective reaction;
参考文献
Lee, Yeon Soo; Hong, Joo Hee; Jeon, Nan Young; Won, Keehoon; Kim, Bum Tae
Organic Process Research and Development, 2004 , vol. 8, # 6 p. 948 - 951
反应条件
immobilized lipase B from Candida antarctica in tert-butyl methyl ether T=65°C; 3 h; Resolution of racemateEnzymatic reaction; Temperature; enantioselective reaction;
参考文献
Lee, Yeon Soo; Hong, Joo Hee; Jeon, Nan Young; Won, Keehoon; Kim, Bum Tae
Organic Process Research and Development, 2004 , vol. 8, # 6 p. 948 - 951
反应条件
immobilized lipase B from Candida antarctica in tert-butyl methyl ether T=65°C; 2 h; Resolution of racemateEnzymatic reaction; Temperature; enantioselective reaction;
参考文献
Lee, Yeon Soo; Hong, Joo Hee; Jeon, Nan Young; Won, Keehoon; Kim, Bum Tae
Organic Process Research and Development, 2004 , vol. 8, # 6 p. 948 - 951
反应条件
sulfuric acid Heating;
参考文献
Pansare, Sunil V.; Ravi, R. Gnana
Tetrahedron Letters, 1995 , vol. 36, # 33 p. 5959 - 5962
反应条件
hydrogen in water; acetic acid P=52505.3 Torr; 1 h; optical yield given as percent eeenantioselective reaction;
参考文献
Keilitz, Juliane; Nowag, Sabrina; Marty, Jean-Daniel; Haag, Rainer
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 9 p. 1503 - 1511
反应条件
hydrogenchloride Reflux;
参考文献
Rioz-Martinez, Ana; Cuetos, Anibal; Rodriguez, Cristina; De Gonzalo, Gonzalo; Lavandera, Ivan; Fraaije, Marco W.; Gotor, Vicente
Angewandte Chemie - International Edition, 2011 , vol. 50, # 36 p. 8387 - 8390