环己基-(4-甲基苯基)甲酮合成路线 (共 14 条)
反应条件
1: diisobutylaluminium hydride / |Inert atmosphere; |Schlenk technique
2: iron tribromide / toluene / 20 h / 110 °C / |Sealed tube; |Schlenk technique; |Inert atmosphere
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参考文献
Gutierrez-Bonet, Alvaro; Flores-Gaspar, Areli; Martin, Ruben
Journal of the American Chemical Society, 2013 , vol. 135, # 34 p. 12576 - 12579
反应条件
europium(III) bis(trifluoromethylsulfonyl)imide
T=250°C; Friedel-Crafts acylation; 24 h; Title compound not separated from byproducts;
参考文献
Kawamura, Masato; Cui, Dong-Mei; Shimada, Shigeru
Tetrahedron, 2006 , vol. 62, # 39 p. 9201 - 9209
反应条件
1: 100 percent / diethyl ether / -78 - 25 °C
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参考文献
Dar; Thiruvazhi; Abraham; Kitayama; Kopajtic; Gamliel; Slusher; Carroll; Uhl
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 10 p. 1013 - 1021
反应条件
[rhenium(pentacarbonyl)(bromide)]
2 h; Heating;
参考文献
Kusama, Hiroyuki; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 8 p. 2379 - 2384