CBZ-L-赖氨酸甲酯盐酸盐合成路线 (共 13 条)
反应条件
aluminium chloride doped on a neutral alumina 0.0233333 h; Irradiation;
参考文献
Bose, D. Subhas; Lakshmiriarayana
Tetrahedron Letters, 1998 , vol. 39, # 31 p. 5631 - 5634
反应条件
thionyl chloride 1 h; 1.) 0 deg C, 1 h, 2.) RT, 20 h;
参考文献
Beck-Piotraschke, Karin; Jakubke, Hans-Dieter
Tetrahedron Asymmetry, 1998 , vol. 9, # 9 p. 1505 - 1518
反应条件
thionyl chloride T=-80 - 20°C; 20 h;
参考文献
Colomer; Pinazo; Manresa; Vinardell; Mitjans; Infante; Perez
Journal of Medicinal Chemistry, 2011 , vol. 54, # 4 p. 989 - 1002
反应条件
1: aqueous NaOH / unter Kuehlung 2: SOCl2 / anschliessend Behandeln mit Methanol View Scheme
参考文献
Su, Jing; Wang, Qiang; Feng, Jinhong; Zhang, Cong; Zhu, Deyu; Wei, Tiandi; Xu, Wenfang; Gu, Lichuan
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 9 p. 2991 - 2996
反应条件
1: aqueous NaOH / unter Kuehlung 2: SOCl2 / anschliessend Behandeln mit Methanol View Scheme
参考文献
Balajthy, Zoltan
Organic Preparations and Procedures International, 1991 , vol. 23, # 3 p. 375 - 376
反应条件
1: SOCl2 / methanol / 30 h / 20 °C 2: 11 g / HCl / 0 °C View Scheme
参考文献
Balajthy, Zoltan
Organic Preparations and Procedures International, 1991 , vol. 23, # 3 p. 375 - 376
反应条件
1.1: NaOH; CuSO4*5H2O; NaHCO3 / H2O / 3 h / 0 °C 1.2: 80 percent / EDTA; conc. HCl / H2O / pH 7.0 2.1: SOCl2 / methanol / 30 h / 20 °C 3.1: 11 g / HCl / 0 °C View Scheme
参考文献
Balajthy, Zoltan
Organic Preparations and Procedures International, 1991 , vol. 23, # 3 p. 375 - 376
反应条件
hydrogenchloride T=0°C; Esterification;
参考文献
Balajthy, Zoltan
Organic Preparations and Procedures International, 1991 , vol. 23, # 3 p. 375 - 376
反应条件
thionyl chloride anschliessend Behandeln mit Methanol;
参考文献
Boissonnas et al.
Helvetica Chimica Acta, 1958 , vol. 41, p. 1867,1876
反应条件
1: sodium hydroxide / tetrahydrofuran; water 2: hydrogen; palladium on activated charcoal / methanol View Scheme
参考文献
Quitterer, Felix; Beck, Philipp; Bacher, Adelbert; Groll, Michael
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 7033 - 7037
Angew. Chem., 2013 , vol. 125, # 27 p. 7171 - 7175,5